Sintesis dan Analisis Spektra IR, Difraktogram XRD, SEM pada Material Katalis Berbahan Ni/zeolit Alam Teraktivasi dengan Metode Impregnasi

Abstract

This research is about the synthesis and analysis of IR spectra, XRD difractogram, SEM in the catalyst material made from Ni/zeolite nature is activated by impregnation method. This study is aimed to find out  (1) The method of  synthesis of catalyst Ni/zeolit with impregnation (2) The characteristics of the catalyst which is formed from the characterization results using SEM, FT-IR, and XRD (3) the optimum ratio of zeolit and Ni in the synthesis of catalyst Ni/zeolit.

Synthesis of catalyst Ni/zeolit were done by impregnation. Method  with a variety of Ni concentration range 0 %, 5%, and 10%. Characterization of catalyst Ni/zeolit were produced covering the structure morphology and particle size using microgrpahy SEM (Scanning Electron Microscope). While characterization crystallization and the crystal size was performed using diffractogram of XRD (X-Ray Diffraction) and characterization with FT-IR.

From this study it can be concluded that : (1) Ni/zeolit catalyst be synthesized from a solution of Ni(NO₃)₂.6H₂O at variance 0%, 5%, and 10%  with impregnation method, (2) characteristics of Ni/zeolit catalyst were identified using SEM analysis in the form of uneven surface morphology, the XRD, the peaks of Ni/zeolit cryztallinity and FT-IR